Sari, UğurYılmaz, İpekÇukurovalı, A.Güven, KutalmışAksoy, İlhan2020-06-252020-06-252005closedAccess0232-13001521-4079https://doi.org/10.1002/crat.200410416https://hdl.handle.net/20.500.12587/3477The crystal structure of N-[(1Z)-1-(3-methyl-3-phenylcyclobutyl)-2-thiomorpholin-4-ylethylidene] thiourea (C18H26N4S2) has been determined by X-ray crystallographic techniques. The compound crystallizes in the orthorhombic space group Pbca, with unit cell parameters: a = 15.692(3), b = 20.803(8), c = 11.979(6)angstrom, Z = 8, V = 3911(7)angstrom(3). The crystal structure was solved by direct methods and refined by full-matrix least squares to a final R-value of 0.084 for 1447 observed reflections [I > 2 sigma (I)]. In the thiosemicarbazide moiety, the S = C bond length is 1.656(6), N-C-N angle is 115.6(5)degrees. The crystal structure is stabilized by the intermolecular N-H... S hydrogen bonds. (c) 2005 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.eninfo:eu-repo/semantics/closedAccessX-ray crystallographycrystal structurethiosemicarbazonebiological activityArticle40772372610.1002/crat.2004104162-s2.0-25444504789Q3WOS:000230378500016Q3