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Öğe Effect of nickel addition on the microstructure and corrosion resistance properties of porous alumina composites shaped with sugarcane bagasse pore-forming agent(Iop Publishing Ltd, 2019) Dele-Afolabi, T. T.; Hanim, M. A. Azmah; Norkhairunnisa, M.; S Sobri; Calin, R.; Ojo-Kupoluyi, O. J.In this study, the effect of nickel (Ni) addition on the microstructure and corrosion resistance properties of porous alumina (Al2O3) composites shaped with sugarcane bagasse pore-forming agent were evaluated. Plain and Ni-reinforced porous alumina sampels (Al2O3-xNi-RH; x = 2, 4, 6 and 8wt%) were prepared using the powder metallurgy method. Experimental results showed that the porosity (50.4-57.1vol%) and the pore size (62-109 mu m) of the porous alumina composites increased with rising content of Ni reinforcement. The XRD results showed that the Al2O3 matrix and Ni reinforcement reacted during the heat treatment process to produce nickel aluminate (NiAl2O4) spinel. Corrosion resistance results showed that the porous alumina composites exhibited better chemical stability in strong alkali solution as compared with strong acid solution.Öğe Effect of powder size on infiltration height in producing MgO reinforced Al matrix composite by vacuum infiltration method(Trans Tech Publications Ltd, 2007) Çalın, Recep; Citak, RamazanThe vacuum infiltration method is one of the composite producing methods. There are several parameters in composite production by vacuum infiltration. One of them is particle size of reinforcement in particulate reinforced composites. In this study, MgO powder and Al were used as reinforcement and matrix respectively. MgO powders with different size and amount to give same height were filled in quartz tubes and liquid metal was vacuum infiltrated into the MgO powder under same vacuum condition and for same time. Infiltration height was measured and microstructure and fracture behavior of composite were investigated. It has been found that infiltration height and fracture strength were increased with particulate reinforcement sizes. It has also been determined that molten metal temperature facilitates infiltration.Öğe Effect of mg content in matrix on infiltration height in producing MgO/Al composite by vacuum infiltration method(Trans Tech Publications Ltd, 2007) Çalın, Recep; Çıtak, RamazanVacuum infiltration is one of the composite production method. Reinforcement volume ratio, vacuum value, molten matrix composition and temperature, infiltration atmosphere and time are important parameters in infiltration of molten metal into preformed reinforcement. In this study, MgO powder and Al were used as reinforcement and matrix respectively. Mixture of MgO and Al powders with -105 mu n particle size were filled in quartz tubes freely to form 30 % reinforcement volume ratio. Liquid pure Al with varying Mg contents were vacuum infiltrated into the MgO powder under 550 mmHg vacuum at two different temperatures in normal atmosphere for 3 min. After vacuuming, infiltration height and density of produced composite have been determined. Fracture behavior of composites has also been determined by three point fracture test. Microstructure of composites and fracture surface were investigated by SEM analysis. It has been found that fracture strength of composites decreased although infiltration height and density increased with increasing Mg content of liquid Al. It has been also determined that molten metal temperature facilitates infiltration.Öğe Effect of Mg content in matrix on infiltration height in producing MgO/AI composite by vacuum infiltration method(2007) Çalın, Recep; Çıtak, RamazanVacuum infiltration is one of the composite production method. Reinforcement volume ratio, vacuum value, molten matrix composition and temperature, infiltration atmosphere and time are important parameters in infiltration of molten metal into preformed reinforcement. In this study, MgO powder and Al were used as reinforcement and matrix respectively. Mixture of MgO and Al powders with -105 urn particle size were filled in quartz tubes freely to form 30 % reinforcement volume ratio. Liquid pure Al with varying Mg contents were vacuum infiltrated into the MgO powder under 550 mmHg vacuum at two different temperatures in normal atmosphere for 3 min. After vacuuming, infiltration height and density of produced composite have been determined. Fracture behavior of composites has also been determined by three point fracture test. Microstructure of composites and fracture surface were investigated by SEM analysis. It has been found that fracture strength of composites decreased although infiltration height and density increased with increasing Mg content of liquid Al. It has been also determined that molten metal temperature facilitates infiltration.
