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    Formation of Ge nanocrystals and SiGe in PECVD grown SiNx: Ge thin films
    (Elsevier Sci Ltd, 2006) Dana, Aykutlu; Tokay, Serkan; Aydınlı, Atilla
    Formation of Ge nanocrystals in SiNx matrices has been studied using plasma enhanced chemical vapor deposition in both as deposited samples as well as in post-vacuum annealed samples. Low temperature and short duration anneals in vacuum resulted in Ge nanocrystals whereas prolonged anneals at higher temperatures resulted in Ge nanocrystals accompanied with SiGe formation at the SiNx/Si interface. Raman Scattering Spectroscopy was extensively used to track the formation of various phonon modes during the diffusion of Ge through SiNx and into the Si substrate. (C) 2006 Published by Elsevier Ltd.
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    Synthesis and size differentiation of Ge nanocrystals in amorphous SiO 2
    (2006) Ağan, Sedat; Çelik-Aktaş, A.; Zuo, Jian-Min; Dana, Aykutlu; Aydınlı, A.
    Germanosilicate layers were grown on Si substrates by plasma enhanced chemical vapor deposition (PECVD) and annealed at different temperatures ranging from 700-1010 °C for durations of 5 to 60 min. Transmission electron microscopy (TEM) was used to investigate Ge nanocrystal formation in SiO 2:Ge films. High-resolution cross section TEM images, electron energy-loss spectroscopy and energy dispersive X-ray analysis (EDX) data indicate that Ge nanocrystals are present in the amorphous silicon dioxide films. These nanocrystals are formed in two spatially separated layers with average sizes of 15 and 50 nm, respectively. EDX analysis indicates that Ge also diffuses into the Si substrate.
  • Küçük Resim
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    TEM studies of ge nanocrystal formation in PECVD grown SiO2 : Ge/SiO2 multilayers
    (Iop Publishing Ltd, 2006) Agan, Sedat; Dana, Aykutlu; Aydınlı, A.
    We investigate the effect of annealing on the Ge nanocrystal formation in multilayered germanosilicate-oxide films grown on Si substrates by plasma enhanced chemical vapour deposition (PECVD). The multilayered samples were annealed at temperatures ranging from 750 to 900 degrees C for 5 min under nitrogen atmosphere. The onset of formation of Ge nanocrystals, at 750 degrees C, can be observed via high resolution TEM micrographs. The diameters of Ge nanocrystals were observed to be between 5 and 14 nm. As the annealing temperature is raised to 850 degrees C, a second layer of Ge nanocrystals forms next to the original precipitation band, positioning itself closer to the substrate SiO2 interface. High resolution cross section TEM images, electron diffraction and electron energy-loss spectroscopy as well as energy-dispersive x-ray analysis (EDAX) data all indicate that Ge nanocrystals are present in each layer.