Reinvestigation of bromination of 8-substituted quinolines and synthesis of novel phthalonitriles

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dc.contributor.authorOkten, Salih
dc.contributor.authorCakmak, Osman
dc.contributor.authorSaddiqa, Aisha
dc.contributor.authorKeskin, Bahadir
dc.contributor.authorOzdemir, Seda
dc.contributor.authorInal, Merve
dc.date.accessioned2020-06-25T18:16:11Z
dc.date.available2020-06-25T18:16:11Z
dc.date.issued2016
dc.departmentKırıkkale Üniversitesi
dc.descriptionKeskin, Bahadir/0000-0001-8502-8982; Okten, Salih/0000-0001-9656-1803
dc.description.abstractBromination of a series of 8-substituted quinolines was reinvestigated and specified for optimum yields and isolation conditions. Mono bromination of 8-hydroxyquinoline (2a) and 8-aminoquinoline (2c) gave mixture of mono and dibromo derivatives 5,7-dibromo-8-hydroxyquinoline (3a), 5,7-dibromo-8aminoquinoline (3c), 7-bromo-8-hydroxyquinoline (3d), 5-bromo-8-aminoquinoline (3e) while 8methoxyquinoline (2b) furnished 5-bromo-8-methoxyquinoline (3f) as sole product. Novel phthalonitriles, 4(quinolin-8-yloxy) phthalonitrile (6) and 4-chloro-5-(quinolin-8-yloxy) phthalonitrile (8) of 8-hydroxyquinoline (2a) were synthesized and converted into their respective bromo derivatives 4-(5-bromoquinolin-8yloxy) phthalonitrile (7) and 4-((5-bromoquinolin-8-yl) oxy)-5-chlorophthalonitrile (9).en_US
dc.description.sponsorshipScientific and Technological Research Council of Turkey (TUBITAK)Turkiye Bilimsel ve Teknolojik Arastirma Kurumu (TUBITAK) [112T394]; Kirikkale University Research FundKirikkale University [2012/122]; Yildiz Technical UniversityYildiz Technical University [2015-01-02-GEP01]; Turkey Scholarships program - Government of Turkeyen_US
dc.description.sponsorshipThis study was financially supported by grants from the Scientific and Technological Research Council of Turkey (TUBITAK, Project number: 112T394), Kirikkale University Research Fund (Project number: 2012/122) and Yildiz Technical University (Project number: 2015-01-02-GEP01). Ms. Aisha Saddiqa was awarded a research fellowship by the Turkey Scholarships program, funded by the Government of Turkey, within the scope of this study for one year.en_US
dc.identifier.citationÖkten, Salih & Cakmak, Osman & Saddiqa, Aisha & Keskin, Bahadir & Özdemir, Seda & İnal, Merve. (2016). Reinvestigation of bromination of 8-substituted quinolines and synthesis of novel phthalonitriles. Organic Communications. 9. 82-93.en_US
dc.identifier.endpage93en_US
dc.identifier.issn1307-6175
dc.identifier.issue4en_US
dc.identifier.scopus2-s2.0-85011102795
dc.identifier.scopusqualityQ3
dc.identifier.startpage82en_US
dc.identifier.urihttps://hdl.handle.net/20.500.12587/6447
dc.identifier.volume9en_US
dc.identifier.wosWOS:000411597000002
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherAcg Publicationsen_US
dc.relation.ispartofOrganic Communications
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectBrominationen_US
dc.subjecthydroxyquinolineen_US
dc.subjectphthalonitrileen_US
dc.subjectmethoxyquinolineen_US
dc.subjectaminoquinolineen_US
dc.titleReinvestigation of bromination of 8-substituted quinolines and synthesis of novel phthalonitrilesen_US
dc.typeArticle

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