Preparation and characterization of new nanocomposite polymer films containing NiO nanofillers

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dc.contributor.authorCetinkaya, Sevil
dc.contributor.authorSonmez, Damla
dc.contributor.authorOzker, Taner
dc.date.accessioned2020-06-25T18:29:41Z
dc.date.available2020-06-25T18:29:41Z
dc.date.issued2018
dc.departmentKırıkkale Üniversitesi
dc.description.abstractNanocomposite solid polymer films based on the poly(exo-N-phenyl-7-oxanorbornene-5,6-dicarboximide) (PPhONDI)/LiClO4/NiO system have been designed, and the effect of inorganic NiO nanofiller in different amounts on the film properties has been examined. The exo-PPhONDI/LiClO4/NiO polymer system is the first solid nanocomposite polymer electrolyte film example based on a ring-opening metathesis polymerization (ROMP) host polymer. The NiO nanoparticles were prepared by two-step chemical syntheses, and the thermoplastic host polymer, exo-PPhONDI, was synthesized via ROMP. Composite polymer films were prepared by the solution-casting method. The amount of nanoparticles was varied from 1 to 15wt % of NiO. The conductivity of the nanocomposite solid polymer systems was influenced by the NiO nanofiller concentration. The composite films based on exo-PPhONDI ROMP polymer with the highest conductivity were achieved for the composition with 8 wt % of NiO nanofiller and 10 wt % of LiClO4 dopant. The prepared films were characterized using X-ray diffraction, Fourier transform infrared spectroscopy, differential scanning calorimetry, and scanning electron microscopy (SEM). The SEM results showed that the filler was well distributed in the polymer matrix. (c) 2017 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2018, 135, 45938.en_US
dc.description.sponsorshipKirikkale University Scientific Research Projects Coordination UnitKirikkale University [2013/27]en_US
dc.description.sponsorshipWe thank Kirikkale University Scientific Research Projects Coordination Unit for the financial assistance through the project (project no. 2013/27).en_US
dc.identifier.citationclosedAccessen_US
dc.identifier.doi10.1002/app.45938
dc.identifier.issn0021-8995
dc.identifier.issn1097-4628
dc.identifier.issue12en_US
dc.identifier.scopus2-s2.0-85034742854
dc.identifier.scopusqualityQ2
dc.identifier.urihttps://doi.org/10.1002/app.45938
dc.identifier.urihttps://hdl.handle.net/20.500.12587/7421
dc.identifier.volume135en_US
dc.identifier.wosWOS:000417917200007
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherWileyen_US
dc.relation.ispartofJournal Of Applied Polymer Science
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectcompositesen_US
dc.subjectfilmsen_US
dc.subjectnanostructured polymersen_US
dc.titlePreparation and characterization of new nanocomposite polymer films containing NiO nanofillersen_US
dc.typeArticle

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