Analysis of Phenol in Cigarette Filter Tar Using QuEChERS Sample Preparation and High-Performance Liquid Chromatography/UV Detection System

dc.contributor.authorDemirci, A.
dc.contributor.authorMorkan, B.
dc.date.accessioned2020-06-25T18:07:05Z
dc.date.available2020-06-25T18:07:05Z
dc.date.issued2013
dc.departmentKırıkkale Üniversitesi
dc.description.abstractQuEChERS sample preparation was used for determination of phenol in cigarette filter tar. The method involved extraction with acetonitrile followed by solid-phase extraction cleanup with XAD-4 sorbent and the analyse was carried out with a HPLC-UV equipment. The method was validated using cigarette filter tar spiked at 30-125 mu g cigarette(-1) and the recovery by the method varied from 83 % to 120 % with RSD < 15 %. The method showed good linearity (r(2) = 0.9989) and the LOD was 2.17 mu g cigarette(-1). The amount of phenol found in the filter tar of the three brands of cigarettes were 13.02, 10.23 and 6.08 mu g cigarette(-1), respectively.en_US
dc.description.sponsorshipKirikkale University Scientific Research Project Coordination UnitKirikkale Universityen_US
dc.description.sponsorshipThis study was supported by Kirikkale University Scientific Research Project Coordination Unit.en_US
dc.identifier.citationDemirci, A., & Morkan, B. (2013). Analysis of Phenol in Cigarette Filter Tar Using QuEChERS Sample Preparation and High-Performance Liquid Chromatography/UV Detection System. Asian Journal of Chemistry, 25(12), 6531–6534.en_US
dc.identifier.doi10.14233/ajchem.2013.14330
dc.identifier.endpage6534en_US
dc.identifier.issn0970-7077
dc.identifier.issn0975-427X
dc.identifier.issue12en_US
dc.identifier.scopus2-s2.0-84880075375
dc.identifier.scopusqualityQ4
dc.identifier.startpage6531en_US
dc.identifier.urihttps://doi.org/10.14233/ajchem.2013.14330
dc.identifier.urihttps://hdl.handle.net/20.500.12587/5468
dc.identifier.volume25en_US
dc.identifier.wosWOS:000325088800011
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherAsian Journal Of Chemistryen_US
dc.relation.ispartofAsian Journal Of Chemistry
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectQuEChERSen_US
dc.subjectPhenolen_US
dc.subjectCigaretteen_US
dc.subjectXAD-4en_US
dc.subjectHPLC-UVen_US
dc.titleAnalysis of Phenol in Cigarette Filter Tar Using QuEChERS Sample Preparation and High-Performance Liquid Chromatography/UV Detection Systemen_US
dc.typeArticle

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