Bis(N,N-diethylnicotinamide) p-chlorobenzoate complexes of Ni(II), Zn(II) and Cd(II): SSynthesis and characterization

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dc.contributor.authorKöse, Dursun Ali
dc.contributor.authorGökçe, Gökçehan
dc.contributor.authorGökçe S.
dc.contributor.authorUzun, İbrahim
dc.date.accessioned2020-06-25T15:14:27Z
dc.date.available2020-06-25T15:14:27Z
dc.date.issued2009
dc.departmentKırıkkale Üniversitesi
dc.description.abstractThree novel mixed ligand complexes of Ni(II), Zn(II) and Cd(II) with p-chlorobenzote and N,N-diethylnicotinamide were synthesised and characterized on the basis of elemental analysis, FTIR spectroscopic analysis, solid state UV-Vis spectrometric and magnetic susceptibility data. The thermal behavior of the complexes was studied by simultaneous TG-DTA methods in static air atmosphere and the mass spectra data were recorded. According to microanalytical results, formulas of complexes are C34H40N 4O8ClNi, C34H40N4O 8ClZn and C34H44N4O 10ClCd. The complexes contain two moles of coordination waters, two moles p-chlorobenzoate and two mole N,N-diethylnicotinamide (dena) ligands per formula unit. In these complexes, the p-chlorobenzoate and N,N- diethylnicotinamide behave as monodentate ligand through acidic oxygen and nitrogen of pyridine ring. The decomposition pathways and the stability of the complexes are interpreted in the terms of the structural data. The final decomposition products were found to be as metal oxides. © 2009 Springer Science+Business Media, LLC.en_US
dc.identifier.citationclosedAccessen_US
dc.identifier.doi10.1007/s10973-008-9150-8
dc.identifier.endpage251en_US
dc.identifier.issn13886150
dc.identifier.issue1en_US
dc.identifier.scopus2-s2.0-62949190392
dc.identifier.scopusqualityQ1
dc.identifier.startpage247en_US
dc.identifier.urihttps://doi.org/10.1007/s10973-008-9150-8
dc.identifier.urihttps://hdl.handle.net/20.500.12587/2110
dc.identifier.volume95en_US
dc.identifier.wosWOS:000264326600039
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.relation.ispartofJournal of Thermal Analysis and Calorimetry
dc.relation.publicationcategoryMakale - Ulusal Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectMixed ligand complexesen_US
dc.subjectP-chlorobenzoate N,N-diethylnicotinamideen_US
dc.subjectThermal decompositionen_US
dc.subjectTransition metal complexesen_US
dc.titleBis(N,N-diethylnicotinamide) p-chlorobenzoate complexes of Ni(II), Zn(II) and Cd(II): SSynthesis and characterizationen_US
dc.typeArticle

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