High-yield aqueous synthesis of multi-branched iron oxide core-gold shell nanoparticles: SERS substrate for immobilization and magnetic separation of bacteria

Basit Öğe Kaydı
dc.contributor.authorTamer, Ugur
dc.contributor.authorOnay, Aykut
dc.contributor.authorCiftci, Hakan
dc.contributor.authorBozkurt, Akif Goktug
dc.contributor.authorCetin, Demet
dc.contributor.authorSuludere, Zekiye
dc.contributor.authorGreneche, Jean-Marc
dc.date.accessioned2020-06-25T18:12:07Z
dc.date.available2020-06-25T18:12:07Z
dc.date.issued2014
dc.departmentKırıkkale Üniversitesi
dc.descriptionBayram, Cem/0000-0001-8717-4668; Cetin, Demet/0000-0003-1186-4229; SULUDERE, ZEKIYE/0000-0002-1207-5814; Tamer, Ugur/0000-0001-9989-6123; Greneche, Jean-Marc/0000-0001-7309-8633; Lagarde, Fabienne/0000-0002-4015-4376
dc.description.abstractThe high product yield of multi-branched core-shell Fe3-x O-4@Au magnetic nanoparticles was synthesized used as magnetic separation platform and surface-enhanced Raman scattering (SERS) substrates. The multi-branched magnetic nanoparticles were prepared by a seed-mediated growth approach using magnetic gold nanospheres as the seeds and subsequent reduction of metal salt with ascorbic acid in the presence of a stabilizing agent chitosan biopolymer and silver ions. The anisotropic growth of nanoparticles was observed in the presence of chitosan polymer matrix resulting in multi-branched nanoparticles with a diameter over 100 nm, and silver ions also play a crucial role on the growth of multi-branched nanoparticles. We propose the mechanism of the formation of multi-branched nanoparticles while the properties of nanoparticles embedded in chitosan matrix are discussed. The surface morphology of nanoparticles was characterized with transmission electron microscopy, scanning electron microscopy, ultraviolet visible spectroscopy (UV-Vis), X-ray diffraction, and fourier transform infrared spectroscopy and Fe-57 Mossbauer spectrometry. Additionally, the magnetic properties of the nanoparticles were also examined. We also demonstrated that the synthesized Fe3-x O-4@Au multi-branched nanoparticle is capable of targeted separation of pathogens from matrix and sensing as SERS substrates.en_US
dc.description.sponsorshipScientific and Technological Research Council (TUBITAK)Turkiye Bilimsel ve Teknolojik Arastirma Kurumu (TUBITAK) [108T794, 111T983]; Gazi BAPGazi University [05/2004-03, 05/2011-69]en_US
dc.description.sponsorshipThis work was supported by the Scientific and Technological Research Council (TUBITAK) grant numbers 108T794 and 111T983. We also acknowledge support from Gazi BAP, project number 05/2004-03 and 05/2011-69. We would like to thank Gokhan Demirel and Mehmet Yilmaz for 3D simulation. We also thank to Dr Saime Sebnem Cetin and Prof.Dr. Suleyman Ozcelik for XRD measurements.en_US
dc.identifier.citationclosedAccessen_US
dc.identifier.doi10.1007/s11051-014-2624-7
dc.identifier.issn1388-0764
dc.identifier.issn1572-896X
dc.identifier.issue10en_US
dc.identifier.scopus2-s2.0-84906723005
dc.identifier.scopusqualityQ2
dc.identifier.urihttps://doi.org/10.1007/s11051-014-2624-7
dc.identifier.urihttps://hdl.handle.net/20.500.12587/5739
dc.identifier.volume16en_US
dc.identifier.wosWOS:000341752200001
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherSpringeren_US
dc.relation.ispartofJournal Of Nanoparticle Research
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectMulti-branched iron core-gold shellen_US
dc.subjectChitosanen_US
dc.subjectSERS substrate for immobilizationen_US
dc.subjectMagnetic separation of bacteriaen_US
dc.subjectNanobiotechnologyen_US
dc.titleHigh-yield aqueous synthesis of multi-branched iron oxide core-gold shell nanoparticles: SERS substrate for immobilization and magnetic separation of bacteriaen_US
dc.typeArticle

Dosyalar

Orijinal paket
Listeleniyor 1 - 1 / 1
[ X ]
İsim:
High-yield aqueous synthesis of multi-branched iron oxide core-gold shell nanoparticles SERS substrate for immobilization and magnetic separation of bacteria.pdf
Boyut:
808.3 KB
Biçim:
Adobe Portable Document Format
Açıklama:
Tam Metin/Full Text
İndir

Koleksiyon

WOS İndeksli Yayınlar Koleksiyonu
Makale Koleksiyonu
Scopus İndeksli Yayınlar Koleksiyonu