Preparation and characterization of polyaniline microrods synthesized by using dodecylbenzene sulfonic acid and periodic acid

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dc.contributor.authorTas, Recep
dc.contributor.authorCan, Muzaffer
dc.contributor.authorSonmezoglu, Savas
dc.date.accessioned2020-06-25T18:15:51Z
dc.date.available2020-06-25T18:15:51Z
dc.date.issued2015
dc.departmentKırıkkale Üniversitesi
dc.descriptionSONMEZOGLU, Savas/0000-0002-6011-3504; Tas, Recep/0000-0002-3743-7770
dc.description.abstractThe preparation of polyaniline (PANI) microrod arrays in the presence of dodecylbenzene sulfonic acid (DBSAH), a structure-directing agent, and in the presence of periodic acid (H5IO6), an oxidant in aqua-acidic media, was investigated. DBSAH was performed to distinguish the roles of both surfactant and dopant. The method of preparation of DBSAH and H5IO6 doped PANI (DBSAH-PANI) microrods in a reversed micelle had previously not been reported. The characterizations of the PANI microrods were determined by scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy, (EDX) and X-ray diffraction (XRD). Based on the SEM results, we found that PANI microrods occur in the presence of DBSAH in the polymerization medium, while the XRD results showed that PANI-DBSA gave clearer crystallinity than PANI. At room temperature, the DC conductivities of pure PANI and PANI-DBSA were 9.5 x 10(-2) S/cm and 9.2 x 10(-2) S/cm(-4) x 10(-2) S/cm, respectively, based on the molar ratio of DBSA. The experimental results suggested that it is possible to control both the electrical conductivities and the crystal structures of PANI microrods with DBSAH dopants' incorporation level.en_US
dc.description.sponsorshipScientific Research Commission of Gaziosmanpasa UniversityGaziosmanpasa Universityen_US
dc.description.sponsorshipThe authors want to thank the Scientific Research Commission of Gaziosmanpasa University for its financial support.en_US
dc.identifier.citationTaş R., Can M., Sönmezoğlu S. (2015). Preparation and characterization of polyaniline microrods synthesized by using dodecylbenzene sulfonic acid and periodic acid. Turkish Journal of Chemistry, 39(3), 589 - 599.en_US
dc.identifier.doi10.3906/kim-1411-16
dc.identifier.endpage599en_US
dc.identifier.issn1300-0527
dc.identifier.issue3en_US
dc.identifier.scopus2-s2.0-84938331440
dc.identifier.scopusqualityQ3
dc.identifier.startpage589en_US
dc.identifier.trdizinid171115
dc.identifier.urihttps://doi.org/10.3906/kim-1411-16
dc.identifier.urihttps://hdl.handle.net/20.500.12587/6315
dc.identifier.volume39en_US
dc.identifier.wosWOS:000356077100008
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.indekslendigikaynakTR-Dizin
dc.language.isoen
dc.publisherScientific Technical Research Council Turkey-Tubitaken_US
dc.relation.ispartofTurkish Journal Of Chemistry
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectConducting polymersen_US
dc.subjectpolyanilineen_US
dc.subjectdodecylbenzene sulfonic aciden_US
dc.subjectmicrorodsen_US
dc.titlePreparation and characterization of polyaniline microrods synthesized by using dodecylbenzene sulfonic acid and periodic aciden_US
dc.typeArticle

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