Structural stability of mechanically alloyed amorphous (FeCoNi)70Ti10B20 under high-temperature and high-pressure

dc.authoridozcan, sadan/0000-0001-7966-1845
dc.authoridAvar, Baris/0000-0002-6234-5448
dc.contributor.authorAvar, Baris
dc.contributor.authorSimsek, Tuncay
dc.contributor.authorOzcan, Sadan
dc.contributor.authorChattopadhyay, Arun K.
dc.contributor.authorKalkan, Bora
dc.date.accessioned2025-01-21T16:44:36Z
dc.date.available2025-01-21T16:44:36Z
dc.date.issued2021
dc.departmentKırıkkale Üniversitesi
dc.description.abstractNanostructured (FeCoNi)(70)Ti10B20 (at%) alloy was synthesized by mechanical alloying from elemental powder mixture of Fe, Co, Ni, Ti and B using ball milling. The effect of ball milling time on the evolution of structure and morphology was investigated by X-ray diffraction, scanning and transmission electron microscopy and differential thermal analysis. It was observed that the formation of solid solution of (FeCoNi)(70)Ti10B20 started from the very onset of the milling process. Crystallite size and lattice strains seemed to be leveled off after 20 h of milling with no further major changes. The milling process for longer periods introduced severe plastic deformations causing formation of amorphous phase of (FeCoNi)(70)Ti10B20. The amorphous alloy composition was confirmed by energy dispersive X-ray spectroscopy analysis that showed an excellent homogeneity of the alloying elements. The phase stability of the mechanically alloyed amorphous sample was further verified by employing high-temperature and high-pressure studies. The alloy samples heat-treated at 700 degrees C revealed crystallization of the amorphous phase. However, synchrotron-based high-pressure ambient temperature X-ray diffraction studies confirmed that the amorphous phase of the alloy remained stable up to the pressure of 30 GPa. The 50 h milled sample after being annealed at 350 degrees C showed improvement in the soft magnetic properties of the alloy, which was due to the probable elimination of the residual stress in the amorphous phase of the alloy powders. (C) 2020 Elsevier B.V. All rights reserved.
dc.description.sponsorshipZonguldak Bulent Ecevit University [2015-73338635-01]; COMPRES, the Consortium for Materials Properties Research in Earth Sciences under NSF [EAR 1606856]; Office of Science, Office of Basic Energy Sciences, of the U.S. Department of Energy [DE-AC02-05CH11231]
dc.description.sponsorshipWe would like to thank Zonguldak Bulent Ecevit University (Project no. 2015-73338635-01) for the financial support, Middle East Technical University for TEM measurements, Kastamonu University for VSM measurements, and Zonguldak Bulent Ecevit University, Science and Technology Application and Research Centre for the other characterization measurements. Beamline 12.2.2 at ALS is partially supported by COMPRES, the Consortium for Materials Properties Research in Earth Sciences under NSF Cooperative Agreement EAR 1606856. The Advanced Light Source is supported by the Director, Office of Science, Office of Basic Energy Sciences, of the U.S. Department of Energy under Contract No. DE-AC02-05CH11231.
dc.identifier.doi10.1016/j.jallcom.2020.158528
dc.identifier.issn0925-8388
dc.identifier.issn1873-4669
dc.identifier.scopus2-s2.0-85099064728
dc.identifier.scopusqualityQ1
dc.identifier.urihttps://doi.org/10.1016/j.jallcom.2020.158528
dc.identifier.urihttps://hdl.handle.net/20.500.12587/25493
dc.identifier.volume860
dc.identifier.wosWOS:000614154600125
dc.identifier.wosqualityQ1
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherElsevier Science Sa
dc.relation.ispartofJournal of Alloys and Compounds
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/openAccess
dc.snmzKA_20241229
dc.subjectMechanical alloying; Amorphous; High-pressure; Alloy; Soft magnetic behavior
dc.titleStructural stability of mechanically alloyed amorphous (FeCoNi)70Ti10B20 under high-temperature and high-pressure
dc.typeArticle

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