Crystal structure of N-[(1Z)-1-(3-methyl-3-phenyleyclobutyl)-2-thiomorpholin-4-ylethylidene] thiourea

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dc.contributor.authorSari, Uğur
dc.contributor.authorYılmaz, İpek
dc.contributor.authorÇukurovalı, A.
dc.contributor.authorGüven, Kutalmış
dc.contributor.authorAksoy, İlhan
dc.date.accessioned2020-06-25T17:40:32Z
dc.date.available2020-06-25T17:40:32Z
dc.date.issued2005
dc.departmentKırıkkale Üniversitesi
dc.description.abstractThe crystal structure of N-[(1Z)-1-(3-methyl-3-phenylcyclobutyl)-2-thiomorpholin-4-ylethylidene] thiourea (C18H26N4S2) has been determined by X-ray crystallographic techniques. The compound crystallizes in the orthorhombic space group Pbca, with unit cell parameters: a = 15.692(3), b = 20.803(8), c = 11.979(6)angstrom, Z = 8, V = 3911(7)angstrom(3). The crystal structure was solved by direct methods and refined by full-matrix least squares to a final R-value of 0.084 for 1447 observed reflections [I > 2 sigma (I)]. In the thiosemicarbazide moiety, the S = C bond length is 1.656(6), N-C-N angle is 115.6(5)degrees. The crystal structure is stabilized by the intermolecular N-H... S hydrogen bonds. (c) 2005 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.en_US
dc.identifier.citationclosedAccessen_US
dc.identifier.doi10.1002/crat.200410416
dc.identifier.endpage726en_US
dc.identifier.issn0232-1300
dc.identifier.issn1521-4079
dc.identifier.issue7en_US
dc.identifier.scopus2-s2.0-25444504789
dc.identifier.scopusqualityQ3
dc.identifier.startpage723en_US
dc.identifier.urihttps://doi.org/10.1002/crat.200410416
dc.identifier.urihttps://hdl.handle.net/20.500.12587/3477
dc.identifier.volume40en_US
dc.identifier.wosWOS:000230378500016
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherWiley-V C H Verlag Gmbhen_US
dc.relation.ispartofCrystal Research And Technology
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectX-ray crystallographyen_US
dc.subjectcrystal structureen_US
dc.subjectthiosemicarbazoneen_US
dc.subjectbiological activityen_US
dc.titleCrystal structure of N-[(1Z)-1-(3-methyl-3-phenyleyclobutyl)-2-thiomorpholin-4-ylethylidene] thioureaen_US
dc.typeArticle

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